Alloy formation at the Ni-Al interface for Ni films deposited on Al(110) surfaces

V.Shutthanandana, Adli A. Saleh, and R. J. Smith,
Department of Physics, Montana State University, Bozeman, Montana 59717*



Alloy formation at the Ni-Al interface for thin Ni films deposited on Al(110) surfaces has been studied using high-energy ion scattering/channeling (HEIS) and x-ray photoelectron spectroscopy (XPS).  For Ni atoms deposited at room temperature on Al(110) a large amount of Ni-Al intermixing occurs at the interface.  For the first two monolayers (ML) of deposited Ni, a NiAl-like compound is formed.  The intermixing continues with a different rate, forming a Ni3Al-like compound for Ni coverages from 2 to 8 ML, at which point a Ni metal film begins to grow on the surface.  Nickel atoms deposited at 250 C on the Al(110) surface exhibit no surface compound formation, but diffuse up to 400Å into the Al substrate.  Interatomic potentials based on the embedded atom method (EAM) are used in a Monte Carlo approach to simulate the evolution of the Ni-Al(110) interface as a function of the Ni coverage.  The calculated ion scattering yields and x-ray photoelectron intensities from Ni and Al atoms in these simulated interfaces are in good quantitative agreement with the experimental results.  The simulations show a high-density Ni-Al alloy forming at the Al(110) surface which apparently inhibits outward diffusion of Al, leading to the more Ni-rich alloy and finally Ni film growth.  The ion scattering simulations show an unusually large amount of backscattering occurring below the Ni-Al(110) interface, apparently associated with defocusing of the incident ion beam.

*Work supported by NSF Grant No. DMR-9710092 and NASA EPSCoR Grant NCCW-0058

Submitted for publication (1999)

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